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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)
 

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Efficient synthesis of butenolide-medium ring ether hybrids by a [3 + 2] cyclization-ring-closing metathesis strategy.

A new strategy for the synthesis of bicyclic gamma-alkylidenebutenolides, butenolide-medium ring ether hybrids, is reported which involves Me(3)SiOTf-catalyzed cyclization of 1, 3-bis(trimethylsilyloxy)-1,3-butadienes with oxalyl chloride, Mitsunobu reaction, and subsequent ring-closing metathesis.[1]

References

  1. Efficient synthesis of butenolide-medium ring ether hybrids by a [3 + 2] cyclization-ring-closing metathesis strategy. Langer, P., Eckardt, T., Stoll, M. Org. Lett. (2000) [Pubmed]
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