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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)
 

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Radical cation of dibenzothiophene fully annelated with bicyclo[2.2.2]octene units: X-ray crystal structure and electronic properties.

New dibenzothiophene 2 fully annelated with bicyclo[2.2.2]octene units was synthesized and oxidized to stable radical cation salt 2(*+)SbCl(6)(-), whose structure was determined by X-ray crystallography. Although the intrinsic electronic structure of 2(*+) is predicted to be close to structure A, an interaction with the counteranion makes structure B contribute significantly. A part of the salt 2(*+)SbCl(6)(-) underwent rearrangement to arenium ion 6(+), whose structure was also clarified by X-ray crystallography.[1]

References

  1. Radical cation of dibenzothiophene fully annelated with bicyclo[2.2.2]octene units: X-ray crystal structure and electronic properties. Yamazaki, D., Nishinaga, T., Komatsu, K. Org. Lett. (2004) [Pubmed]
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