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Klupsch, F. et al.

Major metabolites of zolpidem: expeditious synthesis and mass spectra.

An expeditious route to the two major metabolites of Zolpidem-and readily applicable to the synthesis of the drug-was established via a cyclization reaction between a 2-aminopyridine and a suitable alpha-bromoacetophenone. The structures of the target compounds were confirmed from a 2D (1)H-(15)N NMR correlation. Their mass spectra contribute to a reliable toxicological identification of the drug in the case of drug-facilitated crimes.[1]

References

Major metabolites of zolpidem: expeditious synthesis and mass spectra. Klupsch, F., Houssin, R., Humbert, L., Imbenotte, M., Hénichart, J.P., Lhermitte, M. Chem. Pharm. Bull. (2006) [Pubmed]

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