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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)
 

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Analyses of volatile C2 haloethanes and haloethenes in tissues: sample preparation and extraction.

A tissue extraction procedure was developed which minimized loss of readily volatilizable compounds for subsequent quantification by headspace gas chromatography, and evaluated for perchloroethylene (PER), 1,1,1-trichloroethane, 1,1,2,2-tetrachloroethane, and 1,1,2-trichloroethylene. Of the procedures evaluated, joint isooctane and saline tissue homogenization had the most efficient recovery, ranging from 73 to 104% for the four halocarbons from seven different rat tissues. PER concentrations were also determined in tissues of rats following in vivo halocarbon administration. Recovery did not appear to be tissue-dependent, but did vary somewhat with test chemical, with the least volatile, most lipophilic compounds exhibiting the highest recovery.[1]

References

  1. Analyses of volatile C2 haloethanes and haloethenes in tissues: sample preparation and extraction. Chen, X.M., Dallas, C.E., Muralidhara, S., Srivatsan, V., Bruckner, J.V. J. Chromatogr. (1993) [Pubmed]
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