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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)
 

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Automated flow injection analyzer with on-line solid-phase extraction and chemiluminescence detection for the determination of dodecylamine in diesel fuels.

This paper describes the development of a portable, automated flow injection-chemiluminescence (FI-CL) analyzer incorporating on-line solid-phase extraction (SPE) for the determination of dodecylamine (detergent) in diesel fuels. The method is based on the peroxyoxalate/sulforhodamine 101 chemiluminescence reaction, with SPE required to remove indigenous compounds within the diesel fuel matrix that interfere with the CL response. The automated analyzer achieved a detection limit of 2.9 mg L(-1) and a linear range of 2.9-50 mg L(-1), which was suitable for determinations of dodecylamine at levels typically present in fully formulated diesel fuels (40 mg L(-1)). Analyses of base fuels from five different sources demonstrated that an automated FI-CL-SPE system could provide a portable instrument for monitoring the presence/absence of dodecylamine in diesel fuels.[1]

References

  1. Automated flow injection analyzer with on-line solid-phase extraction and chemiluminescence detection for the determination of dodecylamine in diesel fuels. Fletcher, P.J., Andrew, K.N., Forbes, S., Worsfold, P.J. Anal. Chem. (2003) [Pubmed]
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