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Synthesis of cladobotryal, CJ16,169, and CJ16,170.

Condensation of hydroxypyridone 7 with ethyl pyruvate and p-chlorothiophenol, reduction, and cyclization afforded 77% of lactone 6. Protection of the pyridone, acylation of the enolate with tigloyl chloride, and deprotection provided keto lactone 22. Reduction and dehydrative cyclization completed short and efficient syntheses of 2 and 3.[1]


  1. Synthesis of cladobotryal, CJ16,169, and CJ16,170. Snider, B.B., Che, Q. Org. Lett. (2004) [Pubmed]
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