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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)

Efficient syntheses of rugulosin analogues.

Oxidation of 3b or 14c,d with Pb(OAc)(4) in AcOH for 20 min at 25 degrees C and 1 h at 75 degrees C gave flavoskyrin-type dimers 6b and 15c,d in 53-86% yield. Heating a solution of 6b or 15c,d in pyridine under air for 1 h at 75-80 degrees C and then for 1-2 h at 110 degrees C afforded rugulosin-type dimers 10b and 17c,d in 61-88% yield. This two-step sequence provides a practical route to this unusual natural product skeleton.[1]


  1. Efficient syntheses of rugulosin analogues. Snider, B.B., Gao, X. J. Org. Chem. (2005) [Pubmed]
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