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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)
 
 
 

Efficient total synthesis of (-)-stemoamide.

An efficient diastereoselective synthesis of (-)-stemoamide has been accomplished from a pyroglutamic acid derivative in eight steps and with 24% overall yield. The synthesis features an intramolecular samarium diiodide-promoted 7-exo-trig cyclization of a ketyl radical generated from the corresponding aldehyde.[1]

References

  1. Efficient total synthesis of (-)-stemoamide. Honda, T., Matsukawa, T., Takahashi, K. Org. Biomol. Chem. (2011) [Pubmed]
 
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