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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)
 

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Chemical Compound Review: 

AC1Q1HXA     benzene; hexane

Synonyms: CTK8D9807, AR-1H8214, LS-195639, AC1L37ZE, EINECS 271-738-0, ...
 
 
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High impact information on EINECS 271-738-0

  • The reactions of the aminoalkynes 5, alkynols 7, and alkynylmethines 9 in the presence of Pd2(dba)3 x CHCl3/PhCOOH/renorphos 4 in benzene (or benzene-hexane) at 100 degrees C gave the corresponding cyclization products (nitrogen heterocycles 6, oxygen heterocycles 8, and carbocycles 10) in good yields with good enantioselectivities [1].
  • The esters were crystallized from benzene-hexane, derivatized as trimethylsilyl ethers for gas chromatography on a DB-1 capillary column and for gas chromatography-mass spectrometry with a DB-5 column, and mass spectrometry (MS) in the electron-impact (EI) positive-ion mode at 70 eV [2].

References

  1. Palladium-catalyzed intramolecular asymmetric hydroamination, hydroalkoxylation, and hydrocarbonation of alkynes. Patil, N.T., Lutete, L.M., Wu, H., Pahadi, N.K., Gridnev, I.D., Yamamoto, Y. J. Org. Chem. (2006) [Pubmed]
  2. Pre-column derivatization of free bile acids for high-performance liquid chromatographic and gas chromatographic-mass spectrometric analysis. Ferreira, H.E., Elliott, W.H. J. Chromatogr. (1991) [Pubmed]
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