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Fractionation of moderate molecular weight polysiloxanes by centrifugal TLC.

Fractionation of polydispersed polysiloxanes (1-2 g) into narrow molecular weight fractions has been achieved by a rapid (30-60 min) convenient process, using the Cyclograph Centrifugal Chromatography System. These narrow molecular weight poly(dimethylsiloxane) fractions can be used as secondary standards for GPC.[1]

References

  1. Fractionation of moderate molecular weight polysiloxanes by centrifugal TLC. Gupta, S.K., Sargent, J.R., Weber, W.P. Anal. Chem. (2001) [Pubmed]
 
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