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Yao, Q. et al.

Yao, Kinney, Yang,

Ligand-free Heck reaction: Pd(OAc)2 as an active catalyst revisited.

Palladium acetate was shown to be an extremely active catalyst for the Heck reaction of aryl bromides. Both the base and the solvent were found to have a fundamental influence on the efficiency of the reaction, with K(3)PO(4) and N,N-dimethylacetamide being the optimal base and solvent, respectively.[1]

References

Ligand-free Heck reaction: Pd(OAc)2 as an active catalyst revisited. Yao, Q., Kinney, E.P., Yang, Z. J. Org. Chem. (2003) [Pubmed]

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