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Adsorbed behavior of spin-labeled silane coupling agent on colloidal silica studied by electron spin resonance.

The adsorption mechanism of silane coupling agent on the colloidal silica surface is studied with spin-labeled silane coupling agent using ESR method. The density of the adsorbed silane molecules was determined to be approximately 1.5-2 molecules per 100 A2 of the silica surface in 95% ethanol solution. In addition, ESR signal of spin-labeled agent adsorbed on the colloidal silica surface was composed of two components; slow component attributable to the agents adsorbed directly on the Si--OH groups of the silica surface through hydrogen bond formation and rapid one attributable to the agents interacted with such adsorbed silane molecules.[1]

References

  1. Adsorbed behavior of spin-labeled silane coupling agent on colloidal silica studied by electron spin resonance. Nishiyama, N., Katsuki, H., Horie, K., Asakura, T. J. Biomed. Mater. Res. (1987) [Pubmed]
 
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