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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)
 

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AC polarographic determination of cloxacillin.

Hydrolysis of cloxacillin at pH 4.0 yields an electroactive product which can be determined by polarography. Depending on the concentration of cloxacillin, one of 2 peaks was obtained: The potential ac peaks for a 4.36 mM cloxacillin solution were peak I, -0.23 V and peak II, -0.13 V. For analytical purposes, the first peak was used. A linear relationship was established for levels of cloxacillin between 2.2 X 10(-5) and 2.2 X 10(-3)M. Average recovery was 98.8% (SD 1.8), indicating satisfactory accuracy for the method. Individual capsule and composite assays as well as interference tests are described.[1]

References

  1. AC polarographic determination of cloxacillin. Núñez-Vergara, L.J., Silva, M.M., Squella, J.A. Journal - Association of Official Analytical Chemists. (1982) [Pubmed]
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