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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)
 

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Simultaneous determination of cyclandelate and its metabolite in human plasma by capillary column gas-liquid chromatography.

A method was developed for the simultaneous determination of cyclandelate and mandelic acid concentrations in plasma, involving extraction from plasma followed by trimethylsilylation and chromatography of the derivatives on a glass capillary column with hydrogen flame-ionization detection. Calibration graphs were linear down to at least 20 microgram/ml for each substance. The precision was excellent with a pooled relative standard deviation of 6.3% and 6.4% for cyclandelate and mandelic acid serum samples, respectively. Concentrations below 500 ng/ml of each substance could be detected in human plasma. The method was developed for use in bioavailability and metabolism studies.[1]

References

  1. Simultaneous determination of cyclandelate and its metabolite in human plasma by capillary column gas-liquid chromatography. Andermann, G., Dietz, M. J. Chromatogr. (1981) [Pubmed]
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