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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)
 

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The first example of a seven-coordinate vanadium(III) thiolate complex containing the hydrazine molecule, an intermediate of nitrogen fixation.

The first example of a seven-coordinate vanadium(III) thiolate complex, [V(PS3' ')(N(2)H(4))(3)] (1), where PS3' ' = [P(C(6)H(3)-3-Me(3)Si-2-S)(3)](3)(-), has been synthesized and characterized. Compound 1 contains a tetradentate ligand (PS3' ') and three hydrazine molecules, forming a capped octahedral geometry. A five-coordinate vanadium(III) complex, [V(PS3)(1-Me-Im)] (2), where PS3 = [P(C(6)H(4)-2-S)(3)](3)(-) and 1-Me-Im = 1-methyl-imidazole, was also obtained. Compound 2 adopts a trigonal bipyramidal geometry, in which the vanadium is ligated by the title ligand, PS3, and one 1-Me-Im molecule.[1]

References

  1. The first example of a seven-coordinate vanadium(III) thiolate complex containing the hydrazine molecule, an intermediate of nitrogen fixation. Hsu, H.F., Chu, W.C., Hung, C.H., Liao, J.H. Inorganic chemistry. (2003) [Pubmed]
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