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Hoffmann, R. A wiki for the life sciences where authorship matters. Nature Genetics (2008)

No-D NMR spectroscopy as a convenient method for titering organolithium (RLi), RMgX, and LDA solutions.

[reaction: see text] The concentration of organolithium, organomagnesium halide, and lithium diisopropylamide solutions can be reliably determined using No-D NMR spectroscopy by integration against the added internal standard 1,5-cyclooctadiene (COD) (or cyclooctene). In addition, common impurities and degradation products can be assessed.[1]


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