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Separation and determination of diastereomers of lambda-cyhalothrin by normal phase-liquid chromatography using a CN column.

A simple and rapid normal-phase liquid-chromatographic method for the separation and determination of diastereomers of lambda-cyhalothrin using a CN column and detection at UV-230 nm has been developed. This method has the advantage of totally resolving each of the diastereomers from impurities, such as meta-phenoxy benzaldehyde, cyhalothric acid and cyhalothric acid chloride, of technical and formulated materials, allowing one to monitor the low-temperature conversion of diastereomers of lambda-cyhalothrin for process development.[1]

References

  1. Separation and determination of diastereomers of lambda-cyhalothrin by normal phase-liquid chromatography using a CN column. Rao, R.N., Shankaraiah, B., Sunder, M.S. Analytical sciences : the international journal of the Japan Society for Analytical Chemistry. (2004) [Pubmed]
 
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