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Synthesis and characterization of pyrrolidin-2-one fused N-confused calix[4]phyrins.

[reaction: see text] A facile method for the synthesis of pyrrolidin-2-one fused N-confused calix[4]phyrins is provided by reactions of 5,10,15,20-tetraaryl-2-aza-21-carbaporphyrin with acyl chlorides in the presence of triethylamine. The (1)H NMR and UV-vis spectra of products indicate their loss of macrocyclic aromaticity.[1]

References

  1. Synthesis and characterization of pyrrolidin-2-one fused N-confused calix[4]phyrins. Li, X., Chmielewski, P.J., Xiang, J., Xu, J., Li, Y., Liu, H., Zhu, D. Org. Lett. (2006) [Pubmed]
 
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